Dichloromethane → Ethyl 3-hydroxy-4-trityloxybutanoate

HRID 828897Notes

Reaction equation

HRID 828897 reaction equation
[C:18]([c:19]1[cH:20][cH:21][cH:22][cH:23][cH:24]1)([c:25]1[cH:26][cH:27][cH:28][cH:29][cH:30]1)([c:31]1[cH:32][cH:33][cH:34][cH:35][cH:36]1)[Cl:37].[CH2:38]([Cl:39])[Cl:40].[CH3:11][CH2:12][N:13]([CH2:14][CH3:15])[CH2:16][CH3:17].[CH3:41][N:42]([c:43]1[cH:44][cH:45][n:46][cH:47][cH:48]1)[CH3:49].[OH:1][CH:2]([CH2:3][C:4](=[O:5])[O:6][CH2:7][CH3:8])[CH2:9][OH:10]>>[OH:1][CH:2]([CH2:3][C:4](=[O:5])[O:6][CH2:7][CH3:8])[CH2:9][O:10][C:18]([c:19]1[cH:20][cH:21][cH:22][cH:23][cH:24]1)([c:25]1[cH:26][cH:27][cH:28][cH:29][cH:30]1)[c:31]1[cH:32][cH:33][cH:34][cH:35][cH:36]1

Participants

6

Reactant 5

HCID 6344DichloromethaneHCID 6456Trityl chlorideHCID 8471TriethylamineHCID 142844-(Dimethylamino)pyridineHCID 13978058Ethyl 3,4-dihydroxybutanoate

Product 1

HCID 21924265Ethyl 3-hydroxy-4-trityloxybutanoate

Sources & evidence

ORD record
ord-14a4c2af85d74b3c94f17bc06931c783
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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