Sodium ion → 1-(3-Chloro-5-methoxyphenyl)methanamine

HRID 834016Notes

Reaction equation

HRID 834016 reaction equation
[Al+3:15].[CH2:28]1[O:29][CH2:30][CH2:31][CH2:32]1.[CH3:20][CH2:21][O:22][C:23](=[O:24])[CH3:25].[Cl:1][c:2]1[cH:3][c:4]([CH2:5][N:6]=[N+:7]=[N-:8])[cH:9][c:10]([O:12][CH3:13])[cH:11]1.[H-:14].[H-:17].[H-:18].[H-:19].[Li+:16].[Na+:27].[OH-:26].[OH2:33]>>[Cl:1][c:2]1[cH:3][c:4]([CH2:5][NH2:6])[cH:9][c:10]([O:12][CH3:13])[cH:11]1

Participants

10

Reactant 9

HCID 923Sodium ionHCID 961HydroxideHCID 962WaterHCID 8028TetrahydrofuranHCID 8857Ethyl AcetateHCID 28486Lithium ionHCID 104727Aluminum CationHCID 166653Hydride4×HCID 577398023-Chloro-5-methoxybenzylazide

Product 1

HCID 510637181-(3-Chloro-5-methoxyphenyl)methanamine

Sources & evidence

ORD record
ord-4f3ddf318fb14b1082f8d835bfc339e8
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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