1,2-Dichloroethane → Chloride

HRID 837100Notes

Reaction equation

HRID 837100 reaction equation
[CH2:36]([Cl:37])[CH2:38][Cl:39].[CH3:31][N:32]([CH3:33])[CH:34]=[O:35].[Cl:5][c:6]1[c:7]([S:24][C:25]2([C:28](=[O:29])[OH:30])[CH2:26][CH2:27]2)[cH:8][c:9]([N:13]2[C:14](=[O:23])[C:15]3=[CH:16][CH2:17][CH2:18][CH2:19][CH:20]3[C:21]2=[O:22])[c:10]([F:12])[cH:11]1.[S:1]([Cl:2])([Cl:3])=[O:4]>>[Cl-:3].[Cl:5][c:6]1[c:7]([S:24][C:25]2([C:28](=[O:29])[OH:30])[CH2:26][CH2:27]2)[cH:8][c:9]([N:13]2[C:14](=[O:23])[C:15]3=[CH:16][CH2:17][CH2:18][CH2:19][CH:20]3[C:21]2=[O:22])[c:10]([F:12])[cH:11]1

Participants

6

Reactant 4

HCID 111,2-DichloroethaneHCID 6228DimethylformamideHCID 24386Thionyl ChlorideHCID 678545381-[2-Chloro-4-fluoro-5-(1,2,3,4,5,6-hexahydro-1,3-dioxo-isoindolyl)-phenylthio]-cyclopropanecarboxylic acid

Product 2

HCID 312ChlorideHCID 678545381-[2-Chloro-4-fluoro-5-(1,2,3,4,5,6-hexahydro-1,3-dioxo-isoindolyl)-phenylthio]-cyclopropanecarboxylic acid

Sources & evidence

ORD record
ord-eac18af5282a44c2930cf68524495464
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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