Hydrochloric Acid → Tert-butyl 3-formylazetidine-1-carboxylate

HRID 837211Notes

Reaction equation

HRID 837211 reaction equation
[C:11]([CH3:12])([CH3:13])([CH3:14])[O:15][C:16](=[O:17])[N:18]1[CH2:19][CH:20]([CH2:22][OH:23])[CH2:21]1.[CH2:24]([N:25]([CH2:26][CH3:27])[CH2:28][CH3:29])[CH3:30].[CH2:32]([Cl:33])[Cl:34].[CH3:7][S:8](=[O:9])[CH3:10].[Cl:1][C:2]([C:3]([Cl:4])=[O:5])=[O:6].[ClH:31]>>[C:11]([CH3:12])([CH3:13])([CH3:14])[O:15][C:16](=[O:17])[N:18]1[CH2:19][CH:20]([CH:22]=[O:23])[CH2:21]1

Participants

7

Reactant 6

HCID 313Hydrochloric AcidHCID 679Dimethyl SulfoxideHCID 6344DichloromethaneHCID 8471TriethylamineHCID 65578Oxalyl chlorideHCID 10583745tert-Butyl 3-(hydroxymethyl)azetidine-1-carboxylate

Product 1

HCID 10726182Tert-butyl 3-formylazetidine-1-carboxylate

Sources & evidence

ORD record
ord-37b4e836680a468394b62df4490e7973
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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