HRID889261

反应详情

EQUATION

反应方程式

HRID 889261 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

2-Benzyloxy-4,6-difluoronitrobenzene (1.0 g, 3.77 mmol) is reduced in EtOAc (18 mL) and 100 mg of 5% platinum on carbon under a hydrogen balloon for 6 h. The mixture is filtered through Celite and solvent removed under reduced pressure. The residue is purified by column chromatography to give a yellow liquid as the title compound.

WORKUP

后处理

  1. filtrationThe mixture is filtered through Celite and solvent
  2. customremoved under reduced pressure
  3. customThe residue is purified by column chromatography