HRID910690

反应详情

EQUATION

反应方程式

HRID 910690 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 2,4-dichloropyrimidine (447 mg, 3 mmol) in ethanol (10 mL) was added 1-methylpyperazine (360 mg, 3.6 mmol). The resulting mixture was stirred at room temperature overnight. The resulting white solid was collected by filtration and washed with ethanol, Na2CO3 solution and water and ethanol.

WORKUP

后处理

  1. filtrationThe resulting white solid was collected by filtration
  2. washwashed with ethanol, Na2CO3 solution and water and ethanol