HRID921370

反应详情

EQUATION

反应方程式

HRID 921370 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 6-chloro-N-[4-(dimethylphosphoryl)phenyl]pyrimidin-4-amine (0.072 mmol) in 1.5 mL of ethanol is added 10 L of triethylamine and 1-Methyl piperazine (0.072 mmol). The mixture can be microwaved at 120 degrees. The reaction mixture can then be filtered through a syringe filter and can be purified by prep-HPLC.

WORKUP

后处理

  1. customThe mixture can be microwaved at 120 degrees
  2. filtrationThe reaction mixture can then be filtered through a syringe
  3. filtrationfilter
  4. customcan be purified by prep-HPLC