Sodium ion → 3-(azidomethyl)-1-(4-iodophenyl)-1H-pyrazole

HRID 932351Notes

Reaction equation

HRID 932351 reaction equation
[CH3:43][CH2:44][O:45][C:46]([CH3:47])=[O:48].[Cl:38][C:39]([Cl:40])([Cl:41])[Cl:42].[I:1][c:2]1[cH:3][cH:4][c:5](-[n:8]2[n:9][c:10]([CH3:13])[cH:11][cH:12]2)[cH:6][cH:7]1.[N-:34]=[N+:35]=[N-:36].[N:22]#[C:23][C:24]([N:25]=[N:26][C:27]([C:28]#[N:29])([CH3:30])[CH3:31])([CH3:32])[CH3:33].[Na+:37].[O:14]=[C:15]1[N:16]([Br:17])[C:18](=[O:19])[CH2:20][CH2:21]1.[OH2:49]>>[I:1][c:2]1[cH:3][cH:4][c:5](-[n:8]2[n:9][c:10]([CH2:13][N:34]=[N+:35]=[N-:36])[cH:11][cH:12]2)[cH:6][cH:7]1

Participants

9

Reactant 8

HCID 923Sodium ionHCID 962WaterHCID 5943Carbon TetrachlorideHCID 6547AzobisisobutyronitrileHCID 8857Ethyl AcetateHCID 33558AzideHCID 67184N-bromobutanimideHCID 685095051-(4-iodophenyl)-3-methyl-1H-pyrazole

Product 1

HCID 866140093-(azidomethyl)-1-(4-iodophenyl)-1H-pyrazole

Sources & evidence

ORD record
ord-b57600284fbb42bd9fb488f262c6ca07
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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