Dichloromethane → Benzyl 2-phenyl-2-(tosyloxy)acetate

HRID 936038Notes

Reaction equation

HRID 936038 reaction equation
[CH3:30][CH2:31][N:32]([CH2:33][CH3:34])[CH2:35][CH3:36].[CH3:37][N:38]([CH3:39])[c:40]1[cH:41][cH:42][n:43][cH:44][cH:45]1.[Cl:46][CH2:47][Cl:48].[OH:12][CH:13]([C:14](=[O:15])[O:16][CH2:17][c:18]1[cH:19][cH:20][cH:21][cH:22][cH:23]1)[c:24]1[cH:25][cH:26][cH:27][cH:28][cH:29]1.[c:1]1([CH3:11])[cH:2][cH:3][c:4]([S:7](=[O:8])(=[O:9])[Cl:10])[cH:5][cH:6]1>>[c:1]1([CH3:11])[cH:2][cH:3][c:4]([S:7](=[O:8])(=[O:9])[O:12][CH:13]([C:14](=[O:15])[O:16][CH2:17][c:18]2[cH:19][cH:20][cH:21][cH:22][cH:23]2)[c:24]2[cH:25][cH:26][cH:27][cH:28][cH:29]2)[cH:5][cH:6]1

Participants

6

Reactant 5

HCID 6344DichloromethaneHCID 73974-Toluenesulfonyl chlorideHCID 8471TriethylamineHCID 13461alpha-Hydroxybenzeneacetic acid phenylmethyl esterHCID 142844-(Dimethylamino)pyridine

Product 1

HCID 86618475Benzyl 2-phenyl-2-(tosyloxy)acetate

Sources & evidence

ORD record
ord-0f2472d0cd7545bf84a97521d268d39b
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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