Ammonium → Ethyl 2-(4-bromocyclohexyl)acetate

HRID 944375Notes

Reaction equation

HRID 944375 reaction equation
[Br:25][CH:26]1[CH2:27][CH2:28][C:29](=[O:32])[CH2:30][CH2:31]1.[CH3:15][SiH:16]([CH3:17])[N:18]([CH3:19])[Si:20]([CH3:21])([CH3:22])[CH3:23].[CH3:1][CH2:2][O:3][C:4](=[O:5])[CH2:6][P:7]([O:8][CH2:9][CH3:10])([O:11][CH2:12][CH3:13])=[O:14].[CH3:40][CH2:41][O:42][C:43](=[O:44])[CH3:45].[Cl-:33].[Li:24].[NH4+:34].[O:35]1[CH2:36][CH2:37][CH2:38][CH2:39]1>>[CH3:1][CH2:2][O:3][C:4](=[O:5])[CH2:6][CH:29]1[CH2:28][CH2:27][CH:26]([Br:25])[CH2:31][CH2:30]1

Participants

9

Reactant 8

HCID 223AmmoniumHCID 312ChlorideHCID 8028TetrahydrofuranHCID 8857Ethyl AcetateHCID 13345Triethyl phosphonoacetateHCID 589711N-dimethylsilyl-N-trimethylsilylmethanamineHCID 3028194LithiumHCID 114010884-Bromocyclohexan-1-one

Product 1

HCID 54545940Ethyl 2-(4-bromocyclohexyl)acetate

Sources & evidence

ORD record
ord-580266cea8154f5389e6fb4bb5be6064
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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