4-Methoxybenzyl alcohol → ethyl 2-((N-(butyloxycarbonyl)-N-(p-methoxybenzyl)sulfamoyl)amino)acetate

HRID 946879Notes

Reaction equation

HRID 946879 reaction equation
[CH2:30]([CH2:31][CH2:32][CH3:33])[O:34][C:35](=[O:36])[NH:37][S:38](=[O:39])(=[O:40])[NH:41][CH2:42][C:43](=[O:44])[O:45][CH2:46][CH3:47].[CH2:62]1[O:63][CH2:64][CH2:65][CH2:66]1.[CH3:1][O:2][c:3]1[cH:4][cH:5][c:6]([CH2:9][OH:10])[cH:7][cH:8]1.[O:48]=[C:49]([O:50][CH:51]([CH3:52])[CH3:53])[N:54]=[N:55][C:56]([O:57][CH:58]([CH3:59])[CH3:60])=[O:61].[c:11]1([P:12]([c:13]2[cH:14][cH:15][cH:16][cH:17][cH:18]2)[c:19]2[cH:20][cH:21][cH:22][cH:23][cH:24]2)[cH:25][cH:26][cH:27][cH:28][cH:29]1>>[CH3:1][O:2][c:3]1[cH:4][cH:5][c:6]([CH2:9][N:37]([C:35]([O:34][CH2:30][CH2:31][CH2:32][CH3:33])=[O:36])[S:38](=[O:39])(=[O:40])[NH:41][CH2:42][C:43](=[O:44])[O:45][CH2:46][CH3:47])[cH:7][cH:8]1

Participants

6

Reactant 5

HCID 77384-Methoxybenzyl alcoholHCID 8028TetrahydrofuranHCID 11776TriphenylphosphineHCID 75555Diisopropyl diazene-1,2-dicarboxylateHCID 18449914ethyl 2-((N-(butyloxycarbonyl)sulfamoyl)amino)acetate

Product 1

HCID 18449913ethyl 2-((N-(butyloxycarbonyl)-N-(p-methoxybenzyl)sulfamoyl)amino)acetate

Sources & evidence

ORD record
ord-b420cb75084c4e418ce3499ab974d41f
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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