→ HCID 2817096, compound

HRID 962315Notes

Reaction equation

HRID 962315 reaction equation
CC(=O)O.CCO.CCOC(=O)CC(C)=O.NC(N)=O.O.O=Cc1cccnc1.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CCOC(=O)C1=C(C)NC(=O)NC1c1cccnc1

Participants

7

Reactant 0

No Reactant data yet.

Product 1

HCID 2817096HCID 2817096, compoundYield 30%

Reagents, catalysts & solvents 6

HCID 176Acetic AcidOtherHCID 702EthanolOtherHCID 1176UreaOtherHCID 8868Ethyl AcetoacetateOtherHCID 103713-PyridinecarboxaldehydeOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. additionNo procedure recorded
  3. waitNo procedure recorded
  4. filtrationKeep solid
  5. washNo procedure recorded
  6. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-999623768b814c42afaf40a7554beb27
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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