→ HCID 613506, compound

HRID 962317Notes

Reaction equation

HRID 962317 reaction equation
CCO.CCOC(=O)CC(C)=O.NC(N)=O.O.O=Cc1ccco1.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CCOC(=O)C1=C(C)NC(=O)NC1c1ccco1

Participants

6

Reactant 0

No Reactant data yet.

Product 1

HCID 613506HCID 613506, compoundYield 50%

Reagents, catalysts & solvents 5

HCID 702EthanolOther2×HCID 1176UreaOtherHCID 7362FurfuralOtherHCID 8868Ethyl AcetoacetateOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
100 °C

Workup

  1. waitNo procedure recorded
  2. filtrationKeep solid
  3. washNo procedure recorded
  4. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-256fb691c2464412ba5eb582919034e6
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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