→ HCID 296188, compound

HRID 962334Notes

Reaction equation

HRID 962334 reaction equation
CCO.COC(=O)CC(OC)OC.NC(N)=O.O.O=Cc1ccccc1.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>COC(=O)C1=C(C)NC(=O)NC1c1ccccc1

Participants

6

Reactant 0

No Reactant data yet.

Product 1

HCID 296188HCID 296188, compoundYield 31%

Reagents, catalysts & solvents 5

HCID 240BenzaldehydeOtherHCID 702EthanolOther2×HCID 1176UreaOtherHCID 81924Methyl 3,3-dimethoxypropionateOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. filtrationKeep solid
  3. washNo procedure recorded
  4. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-59350edb164445468aeb7ab7eb6a8124
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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