→ HCID 3114344, compound

HRID 962335Notes

Reaction equation

HRID 962335 reaction equation
C1COCCO1.CCO.COC(=O)CC(OC)OC.COc1cc(C=O)cc(OC)c1OC.NC(N)=O.[Cl-].[H+]>>COC(=O)C1=C(C)NC(=O)NC1c1cc(OC)c(OC)c(OC)c1

Participants

7

Reactant 0

No Reactant data yet.

Product 1

HCID 3114344HCID 3114344, compoundYield 31%

Reagents, catalysts & solvents 6

HCID 702EthanolOther2×HCID 1176UreaOtherHCID 68583,4,5-TrimethoxybenzaldehydeOtherHCID 312751,4-DioxaneOtherHCID 81924Methyl 3,3-dimethoxypropionateOtherHCID 183483317647-01-0Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. filtrationKeep solid
  3. washNo procedure recorded
  4. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-8eed243f76c9469782234b436a6346b5
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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