→ HCID 13640358, compound

HRID 962342Notes

Reaction equation

HRID 962342 reaction equation
C1COCCO1.CC(=O)CC(N)=O.CCO.NC(=S)Nc1ccccc1.O=Cc1ccccc1.[Cl-].[H+]>>CC1=C(C(N)=O)C(c2ccccc2)NC(=S)N1c1ccccc1

Participants

7

Reactant 0

No Reactant data yet.

Product 1

HCID 13640358HCID 13640358, compoundYield 21%

Reagents, catalysts & solvents 6

HCID 240BenzaldehydeOtherHCID 702EthanolOther2×HCID 312751,4-DioxaneOtherHCID 80077AcetoacetamideOtherHCID 676454PhenylthioureaOtherHCID 183483317647-01-0Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. filtrationKeep solid
  3. washNo procedure recorded
  4. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-e27d1363901440b48f02db93ee0f5b66
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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