→ HCID 3313593, compound

HRID 962343Notes

Reaction equation

HRID 962343 reaction equation
C1COCCO1.CC(=O)CC(N)=O.CCO.NC(N)=O.O=Cc1ccc([N+](=O)[O-])cc1.[Cl-].[H+]>>CC1=C(C(N)=O)C(c2ccc([N+](=O)[O-])cc2)NC(=O)N1

Participants

7

Reactant 0

No Reactant data yet.

Product 1

HCID 3313593HCID 3313593, compoundYield 59%

Reagents, catalysts & solvents 6

HCID 5414-NitrobenzaldehydeOtherHCID 702EthanolOther2×HCID 1176UreaOtherHCID 312751,4-DioxaneOtherHCID 80077AcetoacetamideOtherHCID 183483317647-01-0Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. filtrationKeep solid
  3. washNo procedure recorded
  4. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-c5893499afa94be4b04e1279020f7b61
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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