HRID963806

反应详情

EQUATION

反应方程式

HRID 963806 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

The method of Example 1 was repeated using zinc powder (2.94 g), copper (I) chloride (0.45 g) molecular sieve 4A (3 g), tetrahydrofuran (54 ml), 1-formyl-1-(3,4-methylenedioxyphenylcyclopropane (3.09 g), acetic anhydride (1.5 ml) and methyl dichlorofluoroacetate (2.36 g) to yield the title compound (2.2 g, 51%).