HRID968459

反应详情

EQUATION

反应方程式

HRID 968459 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A uniform mixture liquid was prepared by mixing 10 g of carbon black particles (average particle size: 30 nm) which were subjected to hydrophobicity-imparting treatment and 1.7 g of azobisisobutyronitrile (AIBN) (polymerization initiator) in 7 g of sodium styrenesulfonate and 130 g of styrene. In a dispersion medium comprising 1800 g of a sodium dodecyl sulfonate aqueous solution (concentration: 0.05 wt. %) and 90 g of calcium phosphate dispersed therein, the uniform mixture liquid was added. The resultant liquid was stirred at 10,000 rpm for 15 minutes by a homogenizer to prepare a suspension. Thereafter, the suspension was subjected to polymerization at 80° C. for 7 hours in a nitrogen atmosphere. After the polymerization, the resultant polymer particles were washed, followed by drying and classification to obtain black particles each comprising carbon black particle coated with (sodium styrene sulfonate-styrene) copolymer. An average particle size of the particles was about 2 microns.

WORKUP

后处理

  1. customA uniform mixture liquid was prepared
  2. additiondispersed
  3. additionthe uniform mixture liquid was added
  4. customto prepare a suspension
  5. customThereafter, the suspension was subjected to polymerization at 80° C. for 7 hours in a nitrogen atmosphere
  6. customAfter the polymerization
  7. washthe resultant polymer particles were washed
  8. customby drying