HRID970838

反应详情

EQUATION

反应方程式

HRID 970838 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In a manner similar to Example 1e, by reacting 4.5 g (21.6 mmol) of 4-allyl-1-ethoxymethoxy-2-methylbenzene with 6.3 g (25.7 mmol) of 9-BBN, 7.4 g (21.6 mmol) of dimethyl 4-trifluoromethanesulphonyloxyphthalate, 5.9 g (42.6 mmol) of potassium carbonate and 880 mg (1.05 mmol) of dichloropalladium diphosphinoferrocene. A yellow oil is obtained (m=7 g, y=80%).

WORKUP

后处理

  1. customA yellow oil is obtained (m=7 g, y=80%)