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HRID975046

反应详情

EQUATION

反应方程式

HRID 975046 的结构方程式

REACTANTS

反应物

3
结构：CC(C)[O-].CC(C)[O-].CC(C)[O-].[Al+3]
HCID11143

2-Propanol, aluminum salt

C9H21AlO3

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：Cc1ncsc1C=O
HCID581339

4-Methyl-1,3-thiazole-5-carbaldehyde

C5H5NOS

PRODUCTS

生成物

1
结构：COCc1scnc1C
HCID11571819

Thiazole, 5-(methoxymethyl)-4-methyl-

C6H9NOS

AUXILIARIES

试剂、催化剂与溶剂

3
结构：CC(C)O
溶剂HCID3776

Isopropanol

C3H8O

结构：CI
溶剂HCID6328

Methyl iodide

CH3I

结构：COCCOC
溶剂HCID8071

未命名化合物

PROCEDURE

实验过程

4-Methyl-5-thiazolecarbaldehyde (J. Amer. Chem. Soc., 1982, 104, 4934-4943) was reduced using aluminium isopropoxide in 2-propanol. The resulting alcohol was treated with sodium hydride in dimethoxyethane and iodomethane was added. Distillation gave the title compound.

WORKUP

后处理

  1. additionwas added
  2. distillationDistillation