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HRID977025

反应详情

EQUATION

反应方程式

HRID 977025 的结构方程式

REACTANTS

反应物

6
结构：CN(C)C=O
HCID6228

N,N-Dimethylformamide

C3H7NO

结构：On1nnc2ccccc21
HCID75771

1-Hydroxybenzotriazole

C6H5N3O

结构：NNC(=O)OCc1ccccc1
HCID79242

Hydrazinecarboxylic acid, phenylmethyl ester

C8H10N2O2

结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：CN(C)C(On1nnc2ccccc21)=[N+](C)C.F[P-](F)(F)(F)(F)F
HCID2733084

Methanaminium, N-[(1H-benzotriazol-1-yloxy)(dimethylamino)methylene]-N-methyl-, hexafluorophosphate(1-) (1:1)

C11H16F6N5OP

结构：COC(=O)COc1ccc(C(=O)O)cc1
HCID13816142

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)COc1ccc(C(=O)NNC(=O)OCc2ccccc2)cc1
HCID19610493

未命名化合物

PROCEDURE

实验过程

In a similar manner to Example 9, starting material step (a), 4-methoxycarbonylmethoxybenzoic acid (580 mg), HBTU (1.04 g), HOBT (420 mg), diisopropylethylamine (1.41 ml), DMF (7.5 ml) and benzyl carbazate (500 mg) were reacted to give benzyl 3-(4-t-butoxycarbonylmethoxybenzoyl)carbazate (550 mg) as an off-white solid; NMR Spectrum (DMSO-d6) 3.70 (3H, s), 4.88 (2H, s), 5.11 (2H, s), 7.03 (2H, d), 7.82 (2H, d), 7.38 (5H, m), 9.28 (1H, br s), 10.20 (1H, br s); Mass Spectrum m/z 359 (M+H)+.

WORKUP

后处理

  1. customwere reacted