HRID979725

反应详情

EQUATION

反应方程式

HRID 979725 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Chromium (II) bis(2-ethylhexanoate) is prepared by the addition of an equimolar mixture of triethylamine and 2-ethylhexanoic acid in heptane to a suspension of 0.5 mole anhydrous chromium (II) chloride in heptane. A slow reaction results in the formation of a deep purple solution and the precipitation of triethylammonium hydrochloride. The product is isolated as a purple oil after removal of the precipitate by filtration and the volatiles under vacuum.

WORKUP

后处理

  1. customA slow reaction
  2. customresults in the formation of a deep purple solution
  3. customthe precipitation of triethylammonium hydrochloride
  4. customThe product is isolated as a purple oil
  5. customafter removal of the precipitate
  6. filtrationby filtration