HRID979725
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Chromium (II) bis(2-ethylhexanoate) is prepared by the addition of an equimolar mixture of triethylamine and 2-ethylhexanoic acid in heptane to a suspension of 0.5 mole anhydrous chromium (II) chloride in heptane. A slow reaction results in the formation of a deep purple solution and the precipitation of triethylammonium hydrochloride. The product is isolated as a purple oil after removal of the precipitate by filtration and the volatiles under vacuum.
WORKUP
后处理
- customA slow reaction
- customresults in the formation of a deep purple solution
- customthe precipitation of triethylammonium hydrochloride
- customThe product is isolated as a purple oil
- customafter removal of the precipitate
- filtrationby filtration