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HRID985844

反应详情

EQUATION

反应方程式

HRID 985844 的结构方程式

REACTANTS

反应物

4
结构：COCC(=O)O
HCID12251

Methoxyacetic acid

C3H6O3

结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：CN(C)C(On1nnc2cccnc21)=[N+](C)C.F[P-](F)(F)(F)(F)F
HCID9886157

Methanaminium, N-((dimethylamino)(3H-1,2,3-triazolo(4,5-b)pyridin-3-yloxy)methylene)-N-methyl-, hexafluorophosphate(1-) (1:1)

C10H15F6N6OP

结构：COc1ccc(C2COCCO2)c2sc(N)nc12
HCID22507697

未命名化合物

PRODUCTS

生成物

1
结构：COCC(=O)Nc1nc2c(OC)ccc(C3COCCO3)c2s1
HCID22507688

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

From methoxyacetic acid, HATU and N-ethyldiisopropylamine in THF, then treatment with (+)-7-[1,4]dioxan-2-yl-4-methoxy-benzothiazol-2-ylamine. [α]D20=+24.9° (c=1.05, CHCl3), ES-MS m/e (%): 339 (M+H+, 100).