2-Methoxybenzaldehyde → HCID 9819512, compound

HRID 988994Notes

Reaction equation

HRID 988994 reaction equation
[NH2:1][C:2]1[CH:7]=[N:6][CH:5]=[CH:4][N:3]=1.[CH3:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([CH3:15])[C:10]=1[N+:16]#[C-:17].[CH3:18][O:19][C:20]1[CH:27]=[CH:26][CH:25]=[CH:24][C:21]=1[CH:22]=O>Cl(O)(=O)(=O)=O>[CH3:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([CH3:15])[C:10]=1[NH:16][C:17]1[N:3]2[CH:4]=[CH:5][N:6]=[CH:7][C:2]2=[N:1][C:22]=1[C:21]1[CH:24]=[CH:25][CH:26]=[CH:27][C:20]=1[O:19][CH3:18]

Participants

5

Reactant 3

HCID 86582-MethoxybenzaldehydeHCID 760092,6-Dimethylphenyl isocyanideHCID 78747Aminopyrazine

Product 1

HCID 9819512HCID 9819512, compound

Reagents, catalysts & solvents 1

HCID 24247Perchloric AcidSolvent

Procedure

Compound (15) was prepared in accordance with general instructions 1 from 1.0 ml aminopyrazine solution (0.1 M, MC), 0.575 ml 2,6-dimethylphenyl isocyanide solution (0.2 M, MC), 0.500 ml 2-methoxybenzaldehyde solution (0.3 M, MC), and 10 μl perchloric acid (w=20%).

Sources & evidence

ORD record
ord-0e5d367a55eb4699a5631553f7fabdc0
Source dataset
uspto-grants-2003_10
Patent number
US06638933B2

Reaction notes

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