Sodium Hydroxide → Zinc sorbate

HRID 421540

Reaktionsgleichung

Reaktionsgleichung von HRID 421540
[OH-].[Na+].[C:3]([OH:10])(=[O:9])/[CH:4]=[CH:5]/[CH:6]=[CH:7]/[CH3:8].[Cl-].[Zn+2:12].[Cl-]>O>[C:3]([O-:10])(=[O:9])/[CH:4]=[CH:5]/[CH:6]=[CH:7]/[CH3:8].[Zn+2:12].[C:3]([O-:10])(=[O:9])/[CH:4]=[CH:5]/[CH:6]=[CH:7]/[CH3:8]

Komponenten

5

Edukt 3

HCID 14798Sodium HydroxideHCID 643460Sorbic AcidHCID 3007855Zincchloride

Produkt 1

HCID 6437346Zinc sorbateAusbeute 76,5 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel2×

Reaktionsbedingungen

Temperatur
70 °C

Versuchsvorschrift

A solution of 47% (w/w) sodium hydroxide (5.5 g) is added to slurry of sorbic acid (5.6 g, 0.05 mol) in water (100 mL) at 70° C. to give a clear slightly alkaline solution. A solution of zinc chloride (3.4 g, 0.025 mol) in water (50 mL) is added and a precipitate is formed immediately. The mixture is stirred at 70° C. for further 2.5 hours. The precipitate is then filtered and dried to yield 5.5 g (76%) zinc sorbate as a fine white powder. IR absorption bands: 1521 and 1418 cm−1.

Aufarbeitung

  1. customto give a clear slightly alkaline solution
  2. customa precipitate is formed immediately
  3. filtrationThe precipitate is then filtered
  4. customdried

Quellen und Nachweise

ORD-Eintrag
ord-db83a7f4caee4815add01ca1209fb291
Quelldatensatz
uspto-grants-2012_01
Patentnummer
US08101544B2

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