Hydroxylamine → Benzohydroxamic acid

HRID 369477

Reaction equation

HRID 369477 reaction equation
[NH2:1][OH:2].C(=O)([O-])O.[Na+].[C:8](Cl)(=[O:15])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>C(OCC)(=O)C>[C:8]([NH:1][OH:2])(=[O:15])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Participants

5

Reactant 3

HCID 787HydroxylamineHCID 7412Benzoyl chlorideHCID 516892Sodium Bicarbonate

Product 1

HCID 10313Benzohydroxamic acid

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

To 156 mg of said compound (16) were added 2 ml of ethyl acetate, 2 ml of aqueous saturated sodium hydrogencarbonate, and 0.042 ml of benzoyl chloride and the mixture was reacted at room temperature for 3 hours to obtain a benzoylamino-alcohol compound (compound (17), C53H65NO14Si, molecular weight of 968.18).

Workup

  1. customthe mixture was reacted at room temperature for 3 hours

Sources & evidence

ORD record
ord-16a1a81cf8bf4ff9a748fcb0588ba26e
Source dataset
uspto-grants-2000_10
Patent number
US06136990

Linked notes

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