反応式
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:9]([O:13]CCCC)(=[O:12])[CH:10]=[CH2:11].C(O)(=O)C=C.C(S)CCCCCCCCCCC.C1(S(OCCCCCCCCCCCC)(=O)=O)C=CC=CC=1.[Na].CCCCCCCCCCCCC1C=CC(S([O-])(=O)=O)=CC=1.CCCCCCCCCCCCC1C=CC=C(S([O-])(=O)=O)C=1.CCCCCCCCCCCCC1C(S([O-])(=O)=O)=CC=CC=1.[Na+].[Na+].[Na+].S(OOS([O-])(=O)=O)([O-])(=O)=O.[NH4+].[NH4+].[OH2:140]>>[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:9]([O:13][CH2:6][CH2:7][CH2:8][CH3:3])(=[O:12])[CH:10]=[CH2:11].[C:3]([OH:12])(=[O:140])[CH:2]=[CH2:1]参加物
反応物 9
生成物 1
実験手順
A styrene/butyl acrylate/acrylic acid latex emulsion is prepared according to the process described in U.S. Pat. No. 5,418,108. In particular, a polymer latex is prepared by the emulsion polymerization of styrene, butyl acrylate and acrylic acid (82/18/2 parts) in a nonionic/anionic surfactant solution as follows. In a reaction vessel are mixed 352 grams of styrene, 48 grams of butyl acrylate, 8 grams of acrylic acid, and 12 grams of dodecanethiol. To the reaction vessel is added 600 milliliters of deionized water in which 9 grams of sodium dodecyl benzene sulfonate anionic surfactant (NEOGEN R™, which contains 60% of active component), 8.6 grams of polyoxyethylene nonyl phenyl ether nonionic surfactant (ANTAROX 8971™, which contains 70% of active component), and 4 grams of ammonium persulfate initiator are dissolved. The resulting emulsion is then polymerized at 70° C. for 8 hours. The resulting latex contains 40% by weight of solids.
後処理
- dissolutionare dissolved
- customThe resulting emulsion is then polymerized at 70° C. for 8 hours
出典と根拠
- ORDレコード
- ord-2b6b13817ddf4ea98bab3d9dd2078c51
- 出典データセット
- uspto-grants-1999_08
- 特許番号
- US05936008
関連ノート
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