反応式
[N+:1]([C:4]1[CH:5]=[N:6][C:7]2[C:12]([CH:13]=1)=[CH:11][CH:10]=[CH:9][CH:8]=2)([O-])=O.C(O)C.C(OCC)(=O)C.[Sn](Cl)Cl>[Pt]=O.[Pd].[Fe].[Zn].C(O)(=O)C.C1COCC1.CO>[NH2:1][C:4]1[CH:5]=[N:6][C:7]2[C:12]([CH:13]=1)=[CH:11][CH:10]=[CH:9][CH:8]=2参加物
12
実験手順
The 3-nitroquinoline derivative of the formula (c) is then catalytically reduced in an inert solvent such as ethanol, ethyl acetate, methanol or THF, using platinum oxide or palladium/carbon, or reduced by iron or zinc and acetic acid or tin (II) chloride, to give the 3-aminoquinoline derivative of the formula (d).
出典と根拠
- ORDレコード
- ord-8821263ce0054d48b38ee0adbffc7235
- 出典データセット
- uspto-grants-1997_12
- 特許番号
- US05693651
関連ノート
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