Dimethyladipate → Disodium adipate

HRID 65824

反応式

HRID 65824 の反応式
[C:1]([O:11]C)(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O:8]C)=[O:7].[OH-].[Na+:14]>C(#N)C>[C:1]([O-:11])(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O-:8])=[O:7].[Na+:14].[Na+:14]

参加物

4

反応物 2

HCID 12329DimethyladipateHCID 14798Sodium Hydroxide

生成物 1

HCID 24073Disodium adipate

試薬・触媒・溶媒 1

HCID 6342Acetonitrile溶媒

実験手順

17.4 g. (0.1 mole) of dimethyl adipate were dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 g. (0.2 mole) of 97% pure sodium hydroxide were added to the reaction mixture as a fine powder (50 mesh). The reaction mixture was stirred at reflux temperature for 18 hours. The resulting solution was filtered hot and the solids were air dried to yield disodium adipate as the reaction product.

後処理

  1. temperatureat reflux temperature for 18 hours
  2. filtrationThe resulting solution was filtered hot
  3. customdried

出典と根拠

ORDレコード
ord-af3c1eef92454c249d5f397014b710cf
出典データセット
uspto-grants-1978_12
特許番号
US04129520

関連ノート

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