Dimethyladipate → Disodium adipate
反応式
[C:1]([O:11]C)(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O:8]C)=[O:7].[OH-].[Na+:14]>C(#N)C>[C:1]([O-:11])(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O-:8])=[O:7].[Na+:14].[Na+:14]参加物
4
実験手順
17.4 g. (0.1 mole) of dimethyl adipate were dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 g. (0.2 mole) of 97% pure sodium hydroxide were added to the reaction mixture as a fine powder (50 mesh). The reaction mixture was stirred at reflux temperature for 18 hours. The resulting solution was filtered hot and the solids were air dried to yield disodium adipate as the reaction product.
後処理
- temperatureat reflux temperature for 18 hours
- filtrationThe resulting solution was filtered hot
- customdried
出典と根拠
- ORDレコード
- ord-af3c1eef92454c249d5f397014b710cf
- 出典データセット
- uspto-grants-1978_12
- 特許番号
- US04129520
反応ノート
読み込み中…