Methyl iodide → HCID 18507447, 화합물
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CO[C:3]([C:5]1[O:6][CH:7]=[C:8]([C:10]#[N:11])[CH:9]=1)=O.[H-].[Na+].CI.[N+]([O-])(O)=O.[NH2:20][C:21]([NH2:23])=[NH:22].[C:24](=[S:26])=S>C1COCC1.CS(C)=O.CN(C=O)C.C(N(CC)CC)C.C(#N)C>[NH2:22][C:21]1[N:23]=[C:3]([C:5]2[O:6][CH:7]=[C:8]([C:10]#[N:11])[CH:9]=2)[C:8]([C:10]#[N:11])=[C:7]([S:26][CH3:24])[N:20]=1참가 물질
11
실험 절차
From 4-cyano-furan-2-carboxylic acid methyl ester with sodium hydride and acetonitrile in THF. Then treatment with sodium hydride, carbon disulphide and methyl iodide in DMSO. Then treatment with guanidine nitrate and triethylamine in DMF. EI-MS m/e (%): 257 (M+, 35), 256 ([M—H]+, 100).
출처 및 근거
- ORD 기록
- ord-9c4531f76dee4585ab286fa6920c1a3b
- 출처 데이터셋
- uspto-grants-2003_07
- 특허 번호
- US06586441B2
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