HRID1088607

反应详情

EQUATION

反应方程式

HRID 1088607 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The hydrochloride product from part (b) (1.81 g., 5 mmole) is partitioned between ethyl acetate and 5% sodium bicarbonate (200 ml. each). The organic layer is washed with brine, dried (MgSO4), and concentrated in vacuo to yield 3-[[(S)-2-amino-1-oxo-3-phenylpropyl]amino]propanoic acid, phenylmethyl ester.

WORKUP

后处理

  1. washThe organic layer is washed with brine
  2. dry with materialdried (MgSO4)
  3. concentrationconcentrated in vacuo