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HRID1355834

反应详情

EQUATION

反应方程式

HRID 1355834 的结构方程式

REACTANTS

反应物

4
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：C#Cc1ccccc1
HCID10821

Phenylacetylene

C8H6

结构：c1ccc(P(c2ccccc2)c2ccccc2)cc1
HCID11776

Triphenylphosphine

C18H15P

结构：N#Cc1c(OS(=O)(=O)C(F)(F)F)nc(N)nc1-c1ccco1
HCID86583747

未命名化合物

PRODUCTS

生成物

1
结构：N#Cc1c(C#Cc2ccccc2)nc(N)nc1-c1ccco1
HCID69782724

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

3
结构：[Cu][I]
催化剂HCID24350

Copper(1+) iodide; Copper(I) iodide; Cuprous iodide; Cuprous iodide (CuI)

CuI

结构：Cl[Pd](Cl)([P](c1ccccc1)(c1ccccc1)c1ccccc1)[P](c1ccccc1)(c1ccccc1)c1ccccc1
催化剂HCID178418476

未命名化合物

结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

From trifluoromethanesulfonic acid 2-amino-5-cyano-6-furan-2-yl-pyrimidin-4-yl ester, phenylacetylene, bis(triphenylphosphine)palladium(II) chloride, triphenylphosphine, triethylamine and copper (I) iodide in THF. EI-MS m/e (%): 286 (M+, 100).