HRID1386020
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Prepared according to the method described in Example 10, from N-boc-1,6-diamino-hexane hydrochloride (0.202 g), 1-hydroxybenzotriazole hydrate (0.065 g), triethylamine (0.11 ml), (2R)-1-[2-(6-(3-propanoic acid)naphthyloxy]-4-(3-pyridyl)-2-butanol (0.147 g, Example 9), dry N,N-dimethylformamide (20 ml) and 1-ethyl-3-(3′-dimethylaminopropyl)carbodiimide hydrochloride (0.092 g) to give the title compound as a pale yellow solid (0.116 g).
WORKUP
后处理
- customPrepared