Chloride → 3-Nitrophenethyl azide

HRID 1554346Notes

Reaction equation

HRID 1554346 reaction equation
[CH3:13][CH2:14][N:15]([CH2:16][CH3:17])[CH2:18][CH3:19].[CH3:20][S:21](=[O:22])(=[O:23])[Cl:24].[Cl-:30].[Cl:33][CH2:34][Cl:35].[I-:32].[Li+:29].[N+:1](=[O:2])([O-:3])[c:4]1[cH:5][c:6]([CH2:7][CH2:8][OH:9])[cH:10][cH:11][cH:12]1.[N-:26]=[N+:27]=[N-:28].[Na+:25].[Na+:31]>>[N+:1](=[O:2])([O-:3])[c:4]1[cH:5][c:6]([CH2:7][CH2:8][N:26]=[N+:27]=[N-:28])[cH:10][cH:11][cH:12]1

Participants

10

Reactant 9

HCID 312ChlorideHCID 923Sodium ion2×HCID 6344DichloromethaneHCID 8471TriethylamineHCID 28486Lithium ionHCID 30165Iodide IonHCID 31297Methanesulfonyl chlorideHCID 33558AzideHCID 1040583-Nitrophenylethyl alcohol

Product 1

HCID 224575343-Nitrophenethyl azide

Sources & evidence

ORD record
ord-96bdbd4401244f41981e042bf7a124da
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (1/10)

Reaction notes

Loading…