反应详情

A mixture of 157 g of 3-bromo-1-chloropropane, 129 g of p-chlorophenol and 165 g of potassium carbonate in 1 liter of acetone is refluxed for 3 days. The mixture is cooled, filtered and the filtrate concentrated under reduced pressure. The residue is distilled to give 184 g of product as an oil, bp 107°-116° C. at 0.5mm.

1. temperatureis refluxed for 3 days
2. temperatureThe mixture is cooled
3. filtrationfiltered
4. concentrationthe filtrate concentrated under reduced pressure
5. distillationThe residue is distilled