Diisopropylamine → HCID 67532332, compound

HRID 185587Notes

Reaction equation

HRID 185587 reaction equation
[CH2:80]1[O:81][CH2:82][CH2:83][CH2:84]1.[CH:23]([NH:24][CH:25]([CH3:26])[CH3:27])([CH3:28])[CH3:29].[Cu:36]([I:37])[I:38].[OH:1][c:2]1[c:3]2[c:4]([c:5]([I:13])[n:6][c:7]1[C:8](=[O:9])[O:10][CH2:11][CH3:12])[c:14](-[c:17]1[cH:18][cH:19][cH:20][cH:21][cH:22]1)[n:15][o:16]2.[Pd:39]([Cl:40])[Cl:41].[Si:30]([CH3:31])([CH3:32])([CH3:33])[C:34]#[CH:35].[c:42]1([P:43]([c:44]2[cH:45][cH:46][cH:47][cH:48][cH:49]2)[c:50]2[cH:51][cH:52][cH:53][cH:54][cH:55]2)[cH:56][cH:57][cH:58][cH:59][cH:60]1.[c:61]1([P:62]([c:63]2[cH:64][cH:65][cH:66][cH:67][cH:68]2)[c:69]2[cH:70][cH:71][cH:72][cH:73][cH:74]2)[cH:75][cH:76][cH:77][cH:78][cH:79]1>>[OH:1][c:2]1[c:3]2[c:4]([c:5]([C:35]#[C:34][Si:30]([CH3:31])([CH3:32])[CH3:33])[n:6][c:7]1[C:8](=[O:9])[O:10][CH2:11][CH3:12])[c:14](-[c:17]1[cH:18][cH:19][cH:20][cH:21][cH:22]1)[n:15][o:16]2

Participants

8

Reactant 7

HCID 7912DiisopropylamineHCID 8028TetrahydrofuranHCID 11776Triphenylphosphine2×HCID 24290Palladium ChlorideHCID 66111TrimethylsilylacetyleneHCID 83717Copper iodideHCID 86648126HCID 86648126, compound

Product 1

HCID 67532332HCID 67532332, compound

Sources & evidence

ORD record
ord-5566d388ebc94d889c31636dd975d355
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (6/10)

Reaction notes

Loading…