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HRID1870201

反应详情

EQUATION

反应方程式

HRID 1870201 的结构方程式

REACTANTS

反应物

4
结构：CN(C)C=O
HCID6228

N,N-Dimethylformamide

C3H7NO

结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CCOC(=O)CN.Cl
HCID2723640

Ethyl glycinate hydrochloride

C4H10ClNO2

结构：Cc1cc([N+](=O)[O-])c(F)cc1F
HCID18695459

1,5-Difluoro-2-methyl-4-nitrobenzene

C7H5F2NO2

PRODUCTS

生成物

1
结构：CCOC(=O)CNc1cc(F)c(C)cc1[N+](=O)[O-]
HCID18695409

未命名化合物

收率 61%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

By using 3.00 g of 2,4-difluoro-5-nitrotoluene, 8.77 g of triethylamine, 40 ml of DMF, 40 ml of THF and 2.42 g of glycine ethyl ester hydrochloride, 2.70 g (61%) of N-(5-fluoro-4-methyl-2-nitrophenyl)glycine ethyl ester was obtained.