HRID1896065

反应详情

EQUATION

反应方程式

HRID 1896065 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of adenine, 1-bromo-3-chloropropane, and potassium carbonate in DMF was stirred at room temperature under argon for 4 days, filtered and evaporated to dryness. The crude product was washed with water and dried. Recrystallization from ethanol gave 9-(3-chloropropyl)adenine.

WORKUP

后处理

  1. filtrationfiltered
  2. customevaporated to dryness
  3. washThe crude product was washed with water
  4. customdried
  5. customRecrystallization from ethanol