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HRID1901193

反应详情

EQUATION

反应方程式

HRID 1901193 的结构方程式

REACTANTS

反应物

4
结构：CN(C)C=O
HCID6228

N,N-Dimethylformamide

C3H7NO

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CC(=O)CBr
HCID11715

Bromoacetone

C3H5BrO

结构：COC(=O)C=Cc1ccc(O)cc1
HCID92203

4-Hydroxycinnamic acid methyl ester

C10H10O3

PRODUCTS

生成物

1
结构：COC(=O)C=Cc1ccc(OCC(C)=O)cc1
HCID53842536

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Following a procedure similar to that described in Preparation 3, but using 16 g of methyl 4-hydroxycinnamate, 14.9 g of bromoacetone, 20 g of potassium carbonate and 150 ml of dimethylformamide, the title compound was obtained as crystals, melting at 117°-118° C. (after recrystallization from ethyl acetate).

WORKUP

后处理

  1. customthat described in Preparation 3