6-Chloro-7-iodo-7-deazapurine → HCID 178525804, compound

HRID 2034658Notes

Reaction equation

HRID 2034658 reaction equation
[Cl:1][c:2]1[c:11]([c:6]2[n:5][cH:4][n:3]1)[c:9]([I:10])[cH:8][nH:7]2.O[CH:12]1[C@H:35]([OH:36])[C@H:33]([OH:34])[C@@H:14]([C@@H:15]([c:25]2[cH:32][c:30]([F:31])[c:28]([Cl:29])[cH:27][cH:26]2)[O:16][C:17]([c:19]3[cH:24][cH:23][cH:22][cH:21][cH:20]3)=[O:18])[O:13]1>>[OH:34][C@@H:33]1[C@@H:14]([C@@H:15]([c:25]2[cH:32][c:30]([F:31])[c:28]([Cl:29])[cH:27][cH:26]2)[O:16][C:17]([c:19]3[cH:24][cH:23][cH:22][cH:21][cH:20]3)=[O:18])[O:13][CH:12]([n:7]4[c:6]([c:11]5[c:9]([I:10])[cH:8]4)[n:5][cH:4][n:3][c:2]5[Cl:1])[C@@H:35]1[OH:36]

Participants

7

Reactant 2

HCID 148092816-Chloro-7-iodo-7-deazapurineHCID 122482768HCID 122482768, compound

Product 1

HCID 178525804HCID 178525804, compound

Reagents, catalysts & solvents 4

HCID 13831TributylphosphineReagentHCID 5363146Diisopropyl azodicarboxylateReagentHCID 6228DimethylformamideSolventHCID 117669-PhenylanthraceneInternal standard

Conditions

Temperature
20 °C

Sources & evidence

ORD record
ord-f392517a13be4f1d86c1118d06dadc2e
Source dataset
39k HTE dataset from Pfizer
Original link
View source

Reaction notes

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