huagongshe.com
HRID20800

反应详情

EQUATION

反应方程式

HRID 20800 的结构方程式

REACTANTS

反应物

4
结构：CCC(=O)CC
HCID7288

3-Pentanone

C5H10O

结构：[C-]#N.[K+]
HCID9032

Potassium cyanide

CKN

结构：CNC.Cl
HCID10473

N-Methylmethanamine hydrochloride

C2H8ClN

结构：CN(C)C1(C#N)CCCC1
HCID10773049

1-(Dimethylamino)cyclopentanecarbonitrile

C8H14N2

PRODUCTS

生成物

1
结构：CCC(C#N)(CC)N(C)C
HCID43802551

未命名化合物

收率 57.5%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

The title compound (8.05 g, 57.5%) was prepared from dimethylamine hydrochloride (8.154 g, 0.1 mol), 3-pentanone (8.61 g, 0.1 mol) and potassium cyanide (6.51 g, 0.1 mol) in water (50 ml) in a similar manner to that described in D1. 1H NMR (CDCl3) δ: 0.96 (6H, t, J=7.6 Hz), 1.67-1.90 (4H, m), 2.33 (6H, s).