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HRID2213983

反应详情

EQUATION

反应方程式

HRID 2213983 的结构方程式

REACTANTS

反应物

7
结构：Cc1ccc(S(=O)(=O)O)cc1
HCID6101

4-Methylbenzenesulfonic acid

C7H8O3S

结构：CC(C)(C#N)N=NC(C)(C)C#N
HCID6547

Azobisisobutyronitrile

C8H12N4

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：NCc1ccccn1
HCID19509

2-Pyridinemethanamine

C6H8N2

结构：BrB(Br)Br
HCID25134

Boron tribromide

BBr3

结构：O=C1CCC(=O)N1Br
HCID67184

1-Bromopyrrolidine-2,5-dione

C4H4BrNO2

结构：Cc1cccc(O)c1N
HCID3014138

2-Amino-m-cresol

C7H9NO

PRODUCTS

生成物

1
结构：COc1cc(O)c(-c2nc3c(CNCc4ccccn4)cccc3o2)cc1OC
HCID135428694

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

5
结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

2 次

结构：CO
溶剂HCID887

Methanol

CH4O

结构：ClC(Cl)(Cl)Cl
溶剂HCID5943

Carbon tetrachloride

CCl4

结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

2 次

PROCEDURE

实验过程

BBr3 in CH2Cl2, rt (b) CH2OCH2Cl, TEA in CH2Cl2, rt (c) amino-m-cresol in benzene, reflux (d) BaMnO4 in benzene, reflux (e) NBS, AIBN in CCl4, reflux (f) 2-aminomethylpyridine derivative, K2CO3 in CH3CN, rt (g) TsOH in CH3OH, rt.