HRID2233743

反应详情

EQUATION

反应方程式

HRID 2233743 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of the product from step (iii) (0.18 g) in EtOAc (30 ml) was added triethylamine (0.15 ml) and 5% Pt/C (36 mg) and the reaction stirred under hydrogen (1 atm) for 2 h. The reaction was filtered through celite and the filtrate evaporated under reduced pressure. Yield 0.139 g.

WORKUP

后处理

  1. filtrationThe reaction was filtered through celite
  2. customthe filtrate evaporated under reduced pressure