HRID23449

反应详情

EQUATION

反应方程式

HRID 23449 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

The title compound was prepared according to General Method 4a using 3-bromofuran (17 mmol), 4-methyl-1-penten-3-ol (25.5 mmol), tetrabutyl ammonium chloride (17 mmol), sodium bicarbonate (42.5 mmol), DMF (15 mL), and palladium acetate (0.9 mmol). The title compound was flash chromatographed eluting with EtOAc:hexane (5:95 to 10:90).

WORKUP

后处理

  1. customThe title compound was prepared
  2. customchromatographed
  3. washeluting with EtOAc:hexane (5:95 to 10:90)