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HRID2403155

反应详情

EQUATION

反应方程式

HRID 2403155 的结构方程式

REACTANTS

反应物

4
结构：C1CCNC1
HCID31268

Pyrrolidine

C4H9N

结构：C[Si](C)(C)C#N
HCID82115

Silanecarbonitrile, trimethyl-

C4H9NSi

结构：CCOC1(O[Si](C)(C)C)CC1
HCID2734686

(1-Ethoxycyclopropoxy)trimethylsilane

C8H18O2Si

结构：CCCCCCC.CCOC(C)=O
HCID21899848

未命名化合物

PRODUCTS

生成物

1
结构：N#CC1(N2CCCC2)CC1
HCID22325146

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

The reaction of (1-ethoxycyclopropoxy)trimethylsilane 13 and pyrrolidine 14D with trimethylsilylcyanide yielded after column chromatography with a gradient of heptane/ethyl acetate (v:v 4:1) to ethyl acetate as solvent 1-(pyrrolidin-1-yl)cyclopropanecarbonitrile as a yellow oil (quant.).