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HRID2406637

反应详情

EQUATION

反应方程式

HRID 2406637 的结构方程式

REACTANTS

反应物

3
结构：[Li+].[OH-]
HCID3939

Lithium hydroxide anhydrous

HLiO

结构：CCOC(C)=O
HCID8857

Ethyl acetate

C4H8O2

结构：CCCCCCc1c(C(=O)CCCC(=O)OC)n(C)c2ccccc12
HCID66643981

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCc1c(C(=O)CCCC(=O)O)n(C)c2ccccc12
HCID49800280

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：O
溶剂HCID962

Water

H2O

结构：CC(C)O
溶剂HCID3776

Isopropanol

C3H8O

PROCEDURE

实验过程

To a solution of 5-(3-hexyl-1-methyl-1H-indol-2-yl)-5-oxo-pentanoic acid methyl ester in isopropanol and water was added LiOH and stirred for 3 hours. The reaction was treated with 1M HCL and ethyl acetate. The product was purified by column chromatography.

WORKUP

后处理

  1. customThe product was purified by column chromatography