Benzoic Acid → HCID 70618390, compound

HRID 2420038Notes

Reaction equation

HRID 2420038 reaction equation
[CH2:1]([O:4][C:5](=[O:13])[NH:6][CH2:7][CH2:8][CH2:9][N:10]([CH3:12])[CH3:11])[CH2:2][CH3:3].[C:14]([OH:22])(=[O:21])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>CCOCC.O1CCCC1>[C:14]([O-:22])(=[O:21])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.[CH2:1]([O:4][C:5](=[O:13])[NH:6][CH2:7][CH2:8][CH2:9][NH+:10]([CH3:11])[CH3:12])[CH2:2][CH3:3]

Participants

5

Reactant 2

HCID 243Benzoic AcidHCID 32490Propamocarb

Product 1

HCID 70618390HCID 70618390, compound

Reagents, catalysts & solvents 2

HCID 3283Diethyl EtherSolventHCID 8028TetrahydrofuranSolvent

Procedure

14.1 g (0.075 mole) of N-(dimethylaminopropyl)-carbamic acid propylester are dissolved in 200 ml of ether. While stirring, 9.15 g (0.075 mole) of benzoic acid in 30 ml of tetrahydrofurane are added in drops. Agitation is continued for 2 hours, the solvent is distilled, and the oil dried in vacuum. One obtains 23.1 g (99.4% of the theory) of nD20 = 1.5070.

Workup

  1. distillationthe solvent is distilled
  2. customthe oil dried in vacuum
  3. customOne obtains 23.1 g (99.4% of the theory) of nD20 = 1.5070

Sources & evidence

ORD record
ord-0972ebc3b72c482d92957f4c8a37e885
Source dataset
uspto-grants-1978_08
Patent number
US04108885

Reaction notes

Loading…