Methylamine → HCID 11668289, compound

HRID 2422577Notes

Reaction equation

HRID 2422577 reaction equation
[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([NH2:11])=[C:6]([CH:10]=1)[C:7]([OH:9])=O.[CH3:12][NH2:13].[CH:14](=O)[C:15]1[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[CH:17][CH:16]=1.Cl[CH2:25][CH2:26][CH2:27]Br.[NH:29]1[CH2:34][CH2:33]C[CH2:31][CH2:30]1>>[CH3:12][N:13]1[C:7](=[O:9])[C:6]2[C:5](=[CH:4][CH:3]=[C:2]([CH3:1])[CH:10]=2)[N:11]=[C:14]1[C:15]1[CH:20]=[CH:19][C:18]([O:21][CH2:22][CH2:31][CH2:30][N:29]2[CH2:34][CH2:33][CH2:27][CH2:26][CH2:25]2)=[CH:17][CH:16]=1

Participants

6

Reactant 5

HCID 6329MethylamineHCID 80061-Bromo-3-chloropropaneHCID 8082PiperidineHCID 312444-MethoxybenzaldehydeHCID 762552-Amino-5-methylbenzoic acid

Product 1

HCID 11668289HCID 11668289, compound

Procedure

The entitled compound was obtained according to the method of Example I but starting from 5-methyl-2-aminobenzoic acid, methylamine, 4-anisaldehyde, 1-chloro-3-bromopropane and piperidine.

Workup

  1. customThe entitled compound was obtained

Sources & evidence

ORD record
ord-dea1e40ea50f4d1899710f6f67ad2454
Source dataset
uspto-grants-2011_06
Patent number
US07960394B2

Reaction notes

Loading…