Methylamine → HCID 11625311, compound
Reaction equation
[CH3:1][C:2]1[C:7]([C:8]([OH:10])=O)=[C:6]([NH2:11])[CH:5]=[CH:4][CH:3]=1.[CH3:12][NH2:13].[CH:14](=O)[C:15]1[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[CH:17][CH:16]=1.Cl[CH2:25][CH2:26][CH2:27]Br.[NH:29]1[CH2:34][CH2:33]C[CH2:31][CH2:30]1>>[CH3:12][N:13]1[C:8](=[O:10])[C:7]2[C:6](=[CH:5][CH:4]=[CH:3][C:2]=2[CH3:1])[N:11]=[C:14]1[C:15]1[CH:20]=[CH:19][C:18]([O:21][CH2:22][CH2:31][CH2:30][N:29]2[CH2:34][CH2:33][CH2:27][CH2:26][CH2:25]2)=[CH:17][CH:16]=1Participants
6
Procedure
The entitled compound was obtained according to the method of Example 1 but starting from 6-methyl-2-aminobenzoic acid, methylamine, 4-anisaldehyde, 1-chloro-3-bromopropane and piperidine.
Workup
- customThe entitled compound was obtained
Sources & evidence
- ORD record
- ord-74fc405c9b7a4b70abb8a4b472eb462e
- Source dataset
- uspto-grants-2011_06
- Patent number
- US07960394B2
Reaction notes
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